Sample introduction systems for the analysis of liquid microsamples by ICP-AES and ICP-MS
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Title: | Sample introduction systems for the analysis of liquid microsamples by ICP-AES and ICP-MS |
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Authors: | Todolí Torró, José Luis | Mermet, Jean Michel |
Research Group/s: | Análisis Químico Aplicado |
Center, Department or Service: | Universidad de Alicante. Departamento de Química Analítica, Nutrición y Bromatología | Laboratoire des Sciences et Stratégies Analytiques |
Keywords: | ICP-AES | ICP–MS | Aerosol transport phenomena | Microsample analysis | Nebulizer | Spray chamber | Desolvation system |
Knowledge Area: | Química Analítica |
Issue Date: | Mar-2006 |
Publisher: | Elsevier |
Citation: | TODOLÍ TORRÓ, José Luis; MERMET, Jean Michel. “Sample introduction systems for the analysis of liquid microsamples by ICP-AES and ICP-MS”. Spectrochimica Acta Part B: Atomic Spectroscopy. Vol. 61, Issue 3 (March 2006). ISSN 0584-8547, pp. 239-283 |
Abstract: | There are many fields in which the available sample volume is the limiting factor for an elemental analysis. Over the last ten years, sample introduction systems used in plasma spectrometry (i.e., Inductively Coupled Plasma Atomic Emission Spectrometry, ICP-AES, and Mass Spectrometry, ICP-MS) have evolved in order to expand the field of applicability of these techniques to the analysis of micro- and nanosamples. A full understanding of the basic processes occurring throughout the sample introduction system is absolutely necessary to improve analytical performance. The first part of the present review deals with fundamental studies concerning the different phenomena taking place from aerosol production to analyte excitation/ionization when the liquid consumption rate does not exceed 100μl/min. Existing sample introduction systems are currently far from the ideal and a significant effort has been made to develop new and efficient devices. Different approaches for continuously introducing small sample volumes (i.e., microsamples) have been reviewed and compared in the present work. Finally, applications as well as basic guidelines to select the best sample introduction system according to the sample particularities are given at the end of this review. |
URI: | http://hdl.handle.net/10045/2752 |
ISSN: | 0584-8547 |
DOI: | 10.1016/j.sab.2005.12.010 |
Language: | eng |
Type: | info:eu-repo/semantics/article |
Peer Review: | si |
Publisher version: | http://dx.doi.org/10.1016/j.sab.2005.12.010 |
Appears in Collections: | INV - AQA-CCA - Artículos de Revistas INV - NANOBIOPOL - Artículos de Revistas |
Files in This Item:
File | Description | Size | Format | |
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sab 2006 (239).pdf | Versión final (acceso restringido) | 1,29 MB | Adobe PDF | Open Request a copy |
Todolí_SAB.pdf | Borrador revisado. Texto (acceso libre) | 452,81 kB | Adobe PDF | Open Preview |
figures.pdf | Borrador revisado. Figuras (acceso libre) | 597,69 kB | Adobe PDF | Open Preview |
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